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in a nonvolatile solvent (HMPA, DMF, DMSO), a large baseline spot will remain because these very polar solvents are poorly eluted. The mobility of the reactants and products might also be affected because of dissolution of these solvents in the eluent as it moves past the baseline spot. However, it may still be possible to follow by TLC reactions in these solvents, especially if they are at least mostly removed following spotting. This can be done by heating with a heat gun and/or pumping off inside a ltering bell jar (Fig. 9.1). The TLC plate is held upright in a small beaker that is placed in the bell. It is good practice to save a small sample of each synthetic intermediate in vials for future TLC comparisons. Authentic samples of the nonvolatile reactants or other known compounds should be spotted on the plate with the reaction mixture to provide more information concerning the identity of a particular spot. This spotting can be done in parallel tracks or even on the same track (called cospotting). The co-spot aids the differentiation of reactants and products when they have similar R fs, and helps diagnose changes in the appearance of the TLC of a reactant when spotted from the reaction mixture. It occasionally happens that a starting material appears different on TLC when spotted from the reaction mixture rather than from a pure sample. This can mislead the chemist into thinking that the starting material has been consumed when it has not.

As with the test drive, the car builder testing approaches can be described by common testing terminology Examine Static testing (observe, read, or review without actually building the car) Perform Functional and structural testing (work different features of the car models, mock-ups, and manufactured subassemblies) Drive Performance testing (work different features of the car in the prototypes) Because you have probably not built a car, it might be helpful to nd examples from a book that details the car-building steps and the manner in which those steps are tested during real car development [8] Example of static testing Read the description of wind tunnel testing that showed changing shapes on the wheel wells would allow the car to achieve 180 mph which became the target speed for road tests later.

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Number of deviations from the standard configuration. Time lag between the availability of the fix and its implementation. Number of software release and distribution methods per platform.

through a linear FIR pre lter, whose lter tap coef cients are carefully designed to generate the desirable synthesized pulse. Section 5.2 describes the spectral properties of the transmitted UWB signal and discusses the pulse design objectives. Section 5.3 introduces the FIR lter structure for UWB waveform synthesis. Section 5.4 focuses on single pulse designs, where the conventional Parks McClellan algorithm [13] is brie y discussed, followed by derivations of optimal convex formulations of the pulse design problem that generate pulses with maximum spectral utilization under the spectral mask constraints. Multiple orthogonal pulse design is addressed via a sequential design strategy in Section 5.5. Design examples are provided in Section 5.6 for single-band, multiband and orthogonal pulses with overlapping spectra, along with comparisons of the spectral utilization ef ciency of various pulses, and evaluation of the system-level impact of pulse shape design in terms of BER performance and robustness to narrowband interference. Concluding remarks are provided in Section 5.7.

Example of test planning Read the estimate of the number of prototypes to be built for testing the C5, around one hundred, compared with the 300 or more expected to be built for normal car pre-production testing These prototypes were expected to be used for all static and dynamic (road) testing prior to the start of assembly line production In fact, some of the prototypes were used to plan and calibrate assembly line production steps Read the description of nal prototype endurance tests that include driving the test car on a closed track at full throttle for a full 24 hours, stopping only for gas and driver changes Examples of functional and structural testing Read the description of heater and air conditioner testing in which drivers would see how soon the heater made things comfortable in freezing weather.

GridFlow [39] is a Grid work ow management system based on ARMS [40] (an agent-based resource management system), Titan [41] (a resource scheduling system) and PACE [42] (a performance prediction tool). Work ow management in GridFlow is performed at multiple layers: Tasks: Tasks are the smallest elements in a work ow. In general, work ow tasks are MPI and PVM jobs running on multiple processors, data transfers to visualization servers or archiving of large data sets to mass storage. Task scheduling is implemented using Titan, which focuses on the sub-work ow and work ow levels of management and scheduling. Sub-work ow: A sub-work ow is a ow of closely related tasks that is to be executed in a prede ned sequence on resources in a local cluster environment. Work ow: A Grid application can be represented as a ow of several different activities, with each activity represented by a sub-work ow. These activities are loosely coupled and may require multi-sited Grid resources.

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